HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-3-nitroaniline → N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-3-nitroaniline | HCID 67768 | — |
| Reactant | 2-Thiophenecarbonyl chloride | HCID 78928 | — |
| Reactant | 3-Fluoro-5-(trifluoromethyl)benzoyl chloride | HCID 519364 | — |
| Product | N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide | HCID 67040567 | — |
Reaction Steps
4-Fluoro-3-nitro-phenylamine was reacted with 3-fluoro-5-trifluoromethyl-benzoyl chloride according to the procedure of Example 256a substituting 3-fluoro-5-trifluoromethyl-benzoyl chloride for thiophene-2-carbonyl chloride to provide N-(4-Fluoro-3-nitro-phenyl)-3-fluoro-5-trifluoromethyl-benzamide which was then reacted according to the procedures of Examples 256b and 256c to provide the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-0c1e77ae6af04c2180c37813f7fe03c7 |
| Source note | uspto-grants-2011_03 |