HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 67040471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | 1,3-Thiazole-2-carbaldehyde | HCID 2734903 | — |
| Reactant | 2-Amino-4-chloro-5-nitrophenol | HCID 3894848 | — |
| Product | HCID 67040471 | HCID 67040471 | 63% |
Reaction Steps
To a flask equipped with a vigreux column was added 2-amino-4-chloro-5-nitro-phenol, thiazole-2-carbaldehyde, Darco KB and xylenes. The mixture was then refluxed overnight and the mixture was cooled, filtered and the solvent removed under vacuum. The resultant solid was recrystallized from Et2O to yield 4.76 g (63%) of a yellow colored solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-f0b4bcb15885449eabf8d59eae0aa0db |
| Source note | uspto-grants-2011_03 |