HCID 67040380, compound → HCID 67041120, compound

Participants

Reaction Steps

The title compound was prepared (yield 88%) by the procedure of Example 385G, substituting the product of Example 447D for the product of Example 385F. 1H-NMR (300 MHz, DMSO-d6) δ ppm: 1.34 (d, J=7.0 Hz, 6H), 3.23 (septet, J=7.0 Hz, 1H), 5.60 (br-s, 2H), 6.05 (quintet, J=9.2 Hz, 1H), 6.63 (d, J=8.5 Hz, 2H), 6.86 (d, J=8.4 Hz, 1H), 7.12 (d, J=8.5 Hz, 2H), 7.36-7.47 (m, 3H), 7.60-7.71 (m, 2H), 7.64 (d, J=8.5 Hz, 1H), 7.75 (br-d, J=8.4 Hz, 1H), 7.95 (br-s, 1H), 8.57 (s, 1H), 8.87 (d, J=8.5 Hz, 1H), 9.42 (d, J=9.5 Hz, 1H), 10.16 (s, 1H) MS ESI+ m/z: 589 (M+H)

Provenance & Evidence