2-Chlorobenzoyl chloride → HCID 67359726, compound

Participants

Reaction Steps

The title compound was prepared using a procedure similar to that of N-(3-cyclopentyl-1-hydroxy-1,3-dihydro-benzo[c][1,2]oxaborol-6-yl)-2-trifluoromethyl-benzamide with 2-chlorobenzoyl chloride replacing 2-trifluoromethylbenzoyl chloride, and with isobutyl magnesium bromide replacing cyclopentyl magnesium bromide. Data: LCMS (M/Z): 344 (M+H); 1H NMR (DMSO-d6) δ: 10.47 (s, 1H), 9.13 (s, 1H), 8.07 (d, J=1.8 Hz, 1H), 7.66 (dd, J=8.2, 2.0 Hz, 1H), 7.51-7.55 (m, 1H), 7.38-7.50 (m, 2H), 7.30 (d, J=8.2 Hz, 1H), 5.10 (dd, J=9.8, 3.0 Hz, 1H), 1.79-1.92 (m, 1H), 1.65 (ddd, J=13.8, 9.0, 3.1 Hz, 1H), 1.26 (ddd, J=14.0, 9.7, 4.7 Hz, 1H), 0.98 (d, J=6.5 Hz, 3H), 0.89 (d, J=6.7 Hz, 3H).

Provenance & Evidence