HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trimethoxybutane → HCID 67041319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trimethoxybutane | HCID 123512 | — |
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 86247649 | HCID 86247649 | — |
| Product | HCID 67041319 | HCID 67041319 | 84.5% |
Reaction Steps
The methods of Part H of Example 35 were used to treat N4-[(5-pyridin-3-ylisoxazol-3-yl)methyl]quinoline-3,4-diamine (0.95 g, 2.98 mmol) with trimethy orthobutyrate (0.57 mL, 3.6 mmol) and pyridine hydrochloride (0.069 g, 0.60 mmol) and purify the product to provide 0.930 g of 2-propyl-1-[(5-pyridin-3-ylisoxazol-3-yl)methyl]-1H-imidazo[4,5-c]quinoline as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915281B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-ae8b79aa40a04ac4a2e150328b1e2d5d |
| Source note | uspto-grants-2011_03 |