4-Bromobenzylamine → HCID 59982332, compound
Reaction equation
[CH:1]1([CH2:4][NH:5][S:6]([C:9]2[CH:14]=[C:13]([Cl:15])[C:12]([O:16][C:17]3[CH:22]=[CH:21][C:20]([N+:23]([O-:25])=[O:24])=[CH:19][C:18]=3[Cl:26])=[C:11]([Cl:27])[CH:10]=2)(=[O:8])=[O:7])[CH2:3][CH2:2]1.[Br:28][C:29]1C=CC(CN)=[CH:31][CH:30]=1>>[Br:28][C:29]1[CH:3]=[CH:2][C:1]([CH2:4][NH:5][S:6]([C:9]2[CH:10]=[C:11]([Cl:27])[C:12]([O:16][C:17]3[CH:22]=[CH:21][C:20]([N+:23]([O-:25])=[O:24])=[CH:19][C:18]=3[Cl:26])=[C:13]([Cl:15])[CH:14]=2)(=[O:8])=[O:7])=[CH:31][CH:30]=1Participants
3
Procedure
This compound was prepared according to the procedure for the preparation of 120 using 4-bromobenzylamine resin in place of the cyclopropylamino methyl resin.
Workup
- customThis compound was prepared
Sources & evidence
- ORD record
- ord-16ac11e35abb480c92f2ba723e8de49b
- Source dataset
- uspto-grants-2011_03
- Patent number
- US07915293B2
Reaction notes
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