HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-1,2,4-Triazole → 3-[3-(1H-1,2,4-triazol-1-yl)propoxy]benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Reactant | 3-(2-Chloroethoxy)benzonitrile | HCID 13569167 | — |
| Reactant | 3-(3-Chloropropoxy)benzonitrile | HCID 21994081 | — |
| Reactant | HCID 178527894 | HCID 178527894 | — |
| Product | 3-[3-(1H-1,2,4-triazol-1-yl)propoxy]benzonitrile | HCID 43289175 | — |
Reaction Steps
By a method similar to that in Reference Example 2, and using, instead of 3-[(2-chloroethyl)oxy]benzonitrile, 3-[(3-chloropropyl)oxy]benzonitrile obtained in Reference Example 4 and using, instead of 1H-1,2,4-triazole-3-thiol, 1H-1,2,4-triazole, the title compound was obtained as a colorless oil (750.0 mg, 32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915267B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-f889fc9bc33b4f7da2e200117161f88f |
| Source note | uspto-grants-2011_03 |