HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-[5-(Methoxyiminomethyl)-pyridin-3-ylethynyl]-benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | 3-(5-Formylpyridin-3-ylethynyl)-benzonitrile | HCID 86076456 | — |
| Product | 3-[5-(Methoxyiminomethyl)-pyridin-3-ylethynyl]-benzonitrile | HCID 86076463 | 75% |
Reaction Steps
Prepare essentially as described in EXAMPLE 6 using methoxylamine hydrochloride (2.88 g, 34.45 mmol), potassium carbonate (2.97 g, 21.53 mmol) and 3-(5-formylpyridin-3-ylethynyl)-benzonitrile (1.00 g, 4.31 mmol), (prepared as described in EXAMPLE 90), to give the title compound (0.84 g, 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-52808d9b03ff42d6b39d44caba368739 |
| Source note | uspto-grants-2011_03 |