HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 67047577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 4-Fluorobenzaldehyde | HCID 68023 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 66631491 | HCID 66631491 | — |
| Product | HCID 67047577 | HCID 67047577 | 54% |
Reaction Steps
trans-4-Amino-2-diphenylmethylpyran 6b (0.24 g, 0.90 mmol) was reacted with 4-fluorobenzaldehyde (0.11 g, 0.90 mmol) in presence of acetic acid (0.05 g, 0.9 mmol), and then reduced with NaCNBH3 (0.07 g, 1.08 mmol) to yield compound 7b (0.18 g, 54%) (Procedure D).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915433B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-dd9bb20ff846468188c95e766af71f5d |
| Source note | uspto-grants-2011_03 |