m-Xylyl bromide → HCID 57469885, compound

HRID 607170Notes

Reaction equation

HRID 607170 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].Br[CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[CH:15]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([CH3:20])[CH:15]=2)=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10]

Participants

3

Reactant 2

HCID 12099m-Xylyl bromideHCID 691274-Chloro-3-nitrophenol

Product 1

HCID 57469885HCID 57469885, compound

Procedure

A solution of 4-chloro-3-nitro-phenol was reacted with 1-Bromomethyl-3-methyl-benzene using the conditions described in Example 10C to provide 1-Chloro-4-(3-methyl-benzyloxy)-2-nitro-benzene which was treated sequentially using the procedures from Examples 10D and 10E to provide the title product.

Sources & evidence

ORD record
ord-3db8fc6658f343d1b579b7b7027cd8ac
Source dataset
uspto-grants-2011_03
Patent number
US07915411B2

Reaction notes

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