4-Chloro-3-nitrophenol → HCID 57469889, compound

HRID 607184Notes

Reaction equation

HRID 607184 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].Cl[CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[C:16]([O:20][CH3:21])[CH:15]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([O:20][CH3:21])[CH:15]=2)=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10]

Participants

3

Reactant 2

HCID 691274-Chloro-3-nitrophenolHCID 699943-Methoxybenzyl chloride

Product 1

HCID 57469889HCID 57469889, compound

Procedure

A solution of 4-chloro-3-nitro-phenol was reacted with 1-Chloromethyl-3-methoxy-benzene using the conditions described in Example 10C to provide 1-Chloro-4-(3-methoxy-benzyloxy)-2-nitro-benzene which was treated sequentially using the procedures from Examples 10D and 10E to provide the title product.

Sources & evidence

ORD record
ord-0ca3a36cae684145a91748e576617c90
Source dataset
uspto-grants-2011_03
Patent number
US07915411B2

Reaction notes

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