4-Chloro-3-nitrophenol → HCID 66809864, compound

HRID 607187Notes

Reaction equation

HRID 607187 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[Cl:12][C:13]1[S:14][C:15]([CH2:18]Cl)=[CH:16][CH:17]=1>>[Cl:12][C:13]1[S:14][C:15]([CH2:18][O:8][C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[C:3]([N+:9]([O-:11])=[O:10])[CH:4]=2)=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 691274-Chloro-3-nitrophenolHCID 5830792-Chloro-5-(chloromethyl)thiophene

Product 1

HCID 66809864HCID 66809864, compound

Procedure

A solution of 4-chloro-3-nitro-phenol was reacted with 2-Chloro-5-chloromethyl-thiophene using the conditions described in Example 10C to provide 2-Chloro-5-(4-chloro-3-nitro-phenoxymethyl)-thiophene which was treated sequentially using the procedures from Examples 10D and 10E to provide the title product.

Sources & evidence

ORD record
ord-b940140716644bcd9230bec8c9df2ba0
Source dataset
uspto-grants-2011_03
Patent number
US07915411B2

Reaction notes

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