HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzaldehyde → 4-[4-(4-Bromo-benzylamino)-2-nitro-phenylsulfanyl]-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 4-(4-Amino-2-nitro-phenylsulfanyl)-phenol | HCID 66808437 | — |
| Product | 4-[4-(4-Bromo-benzylamino)-2-nitro-phenylsulfanyl]-phenol | HCID 66808607 | 73% |
Reaction Steps
A solution of the product from Example 84A and 4-Bromobenzaldehyde were reacted according to the procedure from Example 84B substituting 4-Bromobenzaldehyde for the product from Example 84A to provide the crude product which was purified by silica gel chromatography eluting with 2% methanol in methylene chloride to provide the title compound as a yellow solid (0.11 g, 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915411B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-da4c614ce29040cd8f0dd71e72fce8b9 |
| Source note | uspto-grants-2011_03 |