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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 607221Erstellt: 26. Oktober 2026

2-(4-Methoxy-phenyl)-vinyl-4-methyl-2-nitro-benzene → 2-[2-(4-Methoxy-phenyl)-ethyl]-5-methyl-phenylamine

https://huagongshe.com/reaction/607221

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-(4-Methoxy-phenyl)-vinyl-4-methyl-2-nitro-benzeneHCID 86614623—
EduktHCID 178418361HCID 178418361—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
Produkt2-[2-(4-Methoxy-phenyl)-ethyl]-5-methyl-phenylamineHCID 6680826997%

Reaktionsschritte

To a solution of the product from Example 106A (164 mg, 0.6 mmol) and 10% palladium on charcoal (50 mg) in ethanol (20 ml) was hydrogenated with a hydrogen balloon for three days. The solvent was filtered through celite, washed with ethanol and evaporated under vacuum to provide the title compound (140 mg, 97%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07915411B2
Quelldatensatzuspto-grants-2011_03
ORD IDord-e9f6fd6c8c5c4b6aad6ea28423e4a7c3
Quellennotizuspto-grants-2011_03