HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(4-Methoxy-phenyl)-vinyl-4-methyl-2-nitro-benzene → 2-[2-(4-Methoxy-phenyl)-ethyl]-5-methyl-phenylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(4-Methoxy-phenyl)-vinyl-4-methyl-2-nitro-benzene | HCID 86614623 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2-[2-(4-Methoxy-phenyl)-ethyl]-5-methyl-phenylamine | HCID 66808269 | 97% |
Reaktionsschritte
To a solution of the product from Example 106A (164 mg, 0.6 mmol) and 10% palladium on charcoal (50 mg) in ethanol (20 ml) was hydrogenated with a hydrogen balloon for three days. The solvent was filtered through celite, washed with ethanol and evaporated under vacuum to provide the title compound (140 mg, 97%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07915411B2 |
| Quelldatensatz | uspto-grants-2011_03 |
| ORD ID | ord-e9f6fd6c8c5c4b6aad6ea28423e4a7c3 |
| Quellennotiz | uspto-grants-2011_03 |