HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-nitrotoluene → 4-Ethyl-2-nitro-1-phenylsulfanyl-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-nitrotoluene | HCID 6976 | — |
| Reactant | Sodium benzenethiolate | HCID 4110039 | — |
| Reactant | 1-Chloro-4-ethyl-2-nitro-benzene | HCID 13792156 | — |
| Product | 4-Ethyl-2-nitro-1-phenylsulfanyl-benzene | HCID 57469913 | — |
Reaction Steps
Sodium thiophenolate was reacted with 1-Chloro-4-ethyl-2-nitro-benzene according to the procedure from Example 5H substituting 1-Chloro-4-ethyl-2-nitro-benzene for 4-chloro-3-nitrotoluene to provide 4-Ethyl-2-nitro-1-phenylsulfanyl-benzene which was reduced according to the procedure from Example 5I to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915411B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-54d11cb98c094a3eb4ceb54b11cb6cc4 |
| Source note | uspto-grants-2011_03 |