反应详情

温度

130 °C

A mixture of the product from Example 10B (0.188 g, 1.0 mmol) and 5-bromo-2-(phenylthio)benzenamine (0.280 g, 1.0 mmol) in glacial acetic acid (2 mL) was heated in a 130° C. oil bath for 30 min. The reaction mixture was then cooled to room temperature and the solvent evaporated under reduced pressure. The residue was triturated with methanol, and the resulting solid isolated by vacuum filtration and dried to provide the title compound (0.276 g, 65% yield) as a beige solid.

1. temperatureThe reaction mixture was then cooled to room temperature
2. customthe solvent evaporated under reduced pressure
3. customThe residue was triturated with methanol
4. customthe resulting solid isolated by vacuum filtration
5. customdried