Potassium Hydroxide → HCID 86614629, compound

HRID 607330Notes

Reaction equation

HRID 607330 reaction equation
Cl[C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11].[C:13]([O:17][C:18](=[O:27])[NH:19][C:20]1[CH:25]=[CH:24][C:23]([OH:26])=[CH:22][CH:21]=1)([CH3:16])([CH3:15])[CH3:14].[OH-].[K+]>CS(C)=O>[C:13]([O:17][C:18](=[O:27])[NH:19][C:20]1[CH:21]=[CH:22][C:23]([O:26][C:2]2[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=2[N+:10]([O-:12])=[O:11])=[CH:24][CH:25]=1)([CH3:16])([CH3:14])[CH3:15]

Participants

5

Reactant 3

HCID 14797Potassium HydroxideHCID 855054-Chloro-3-nitrobenzaldehydeHCID 2756771N-Boc-4-hydroxyaniline

Product 1

HCID 86614629HCID 86614629, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

A mixture of 4-chloro-3-nitrobenzaldehyde and (4-Hydroxy-phenyl)-carbamic acid tert-butyl ester were reacted together in DMSO with addition of KOH to provide the title product.

Sources & evidence

ORD record
ord-2b13831ddc7f472e8706b234a7995dae
Source dataset
uspto-grants-2011_03
Patent number
US07915411B2

Reaction notes

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