HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → N-methyl-N-pyridin-2-ylethane-1,2-diamine trifluoroacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Tert-butyl 2-[methyl(pyridin-2-yl)amino]ethylcarbamate | HCID 59216311 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-methyl-N-pyridin-2-ylethane-1,2-diamine trifluoroacetate | HCID 66813129 | — |
Reaction Steps
tert-Butyl 2-[methyl(pyridin-2-yl)amino]ethylcarbamate was stirred with DCM (0.5 ml) and TFA (0.5 ml) for 30 min. The volatiles were removed under reduced pressure to yield the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915408B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-1c33a2ca1ca6438bb46e2785f4c5d3ff |
| Source note | uspto-grants-2011_03 |