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HRID60839

反应详情

EQUATION

反应方程式

HRID 60839 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1cccc2occc12
HCID22324117

1-Benzofuran-4-carboxylic acid

C9H6O3

结构：Cc1nc(C(=O)N2CC3CCCCC3C2CN)c(-c2ccccc2)s1
HCID89740373

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nc(C(=O)N2C[C@H]3CCCC[C@@H]3[C@H]2CNC(=O)c2cccc3occc23)c(-c2ccccc2)s1
HCID89748223

未命名化合物

PROCEDURE

实验过程

The pair of stereo isomers Examples 70 and 71 were isolated by preparative HPLC from the coupling reaction according general procedure A (1-(aminomethyl)-1H-isoindol-2(3H,3aH,4H,5H,6H,7H,7aH)-yl)(2-methyl-5-phenylthiazol-4-yl)methanone and benzofuran-4-carboxylic acid. The assignment of stereochemistry is not verified. MS (ESI) 500 (M+H).

WORKUP

后处理

  1. customThe pair of stereo isomers Examples 70 and 71 were isolated by preparative HPLC from the coupling reaction