HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,4-Dichloropyrimidine → Methyl 2-(2-chloropyrimidin-4-yl)-5-methylbenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Edukt | Methyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate | HCID 46856403 | — |
| Edukt | Methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate | HCID 117727848 | — |
| Produkt | Methyl 2-(2-chloropyrimidin-4-yl)-5-methylbenzoate | HCID 117727617 | — |
Reaktionsschritte
The title compound was synthesized following the same general protocol as described for methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate in Example A1, using methyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate and 2,4-dichloropyrimidine. ESI-MS (m/z): 263 [M+1]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09440982B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-5d81e4ba5f6343f09f530925509d1f00 |
| Quellennotiz | uspto-grants-2016_09 |