HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylboroxine → Methyl 5-methyl-2-(2-methylpyrimidin-4-yl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylboroxine | HCID 574072 | — |
| Reactant | Methyl 2-(2-chloropyrimidin-4-yl)-5-methylbenzoate | HCID 117727617 | — |
| Reactant | Methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate | HCID 117727848 | — |
| Product | Methyl 5-methyl-2-(2-methylpyrimidin-4-yl)benzoate | HCID 117727652 | — |
Reaction Steps
The title compound was synthesized following the same general protocol as described for methyl 5-methyl-2-(1-methyl-1H-pyrazol-4-yl)benzoate in Example A1, using methyl 2-(2-chloropyrimidin-4-yl)-5-methylbenzoate and 2,4,6-trimethyl-1,3,5,2,4,6-trioxatriborinane. ESI-MS (m/z): 243 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440982B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-13cd09cd7bb3491bb93706135f07f125 |
| Source note | uspto-grants-2016_09 |