HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → (2-Fluorophenyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-Fluorophenyl isothiocyanate | HCID 97520 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | (2-Fluorophenyl)thiourea | HCID 2737500 | — |
Reaction Steps
To a stirred solution of 7.0 g (0.045 mol) of 2-fluorophenyl isothiocyanate in 100 ml of ether, was added ammonia gas over a three minute period. A white solid crystallized and was collected by filtration to yield 5.3 g of N-(2- fluorophenyl)thiourea. melting point 147-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998399 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-c8657da7b9344147ac6486e247d11d41 |
| Source note | uspto-grants-1999_12 |