HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorophenyl isocyanate → HCID 15453402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | (+-)-3-Quinuclidinol | HCID 15381 | — |
| Product | HCID 15453402 | HCID 15453402 | 60% |
Reaction Steps
3-Quinuclidinol and 3,4-dichlorophenyl isocyanate were used. Filtration of the precipitated solid from the cooled reaction mixture afforded the title compound (60%) as a white solid: mp 181.0-184.0° C.; FAB LRMS m /z (relative intensity, %) 319 ([MH+ with two Cl37 ], 13), 318 (11), 317 ([MH+ with one Cl37 ], 71), 316 (18), 315 ([MH+ with two Cl35 ], 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998429 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-416d4fbab04f4329860848905f125256 |
| Source note | uspto-grants-1999_12 |