HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-3-Quinuclidinol → HCID 15453401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-3-Quinuclidinol | HCID 15381 | — |
| Reactant | 1-Isocyanato-4-methoxybenzene | HCID 79443 | — |
| Product | HCID 15453401 | HCID 15453401 | 43% |
Reaction Steps
3-Quinuclidinol and 4-methoxyphenyl isocyanate were used. The solid which precipitated from the reaction mixture was recrystallized from ethyl acetate to afford the title compound (43%) as a white solid: mp 159.5-160.5° C.; FAB LRMS m /z (relative intensity, %) 277 (MH+, 16), 110 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998429 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-866cdfc4a545470cbee3200825e46567 |
| Source note | uspto-grants-1999_12 |