HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)-3-Quinuclidinol → HCID 44722650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)-3-Quinuclidinol | HCID 15381 | — |
| Reactant | 3-Methoxyphenyl isocyanate | HCID 87843 | — |
| Product | HCID 44722650 | HCID 44722650 | 60% |
Reaction Steps
3-Quinuclidinol and 3-methoxyphenyl isocyanate were used. The reaction solution was evaporated under reduced pressure, and the residual solid was recrystallized from ethyl acetate to afford the title compound (60%) as a white solid: mp 130.5-132.0° C.; FAB LRMS m /z (relative intensity, %) 278 (18), 277 (MH+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998429 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-1f3a2820c547417d91e293c219453c00 |
| Source note | uspto-grants-1999_12 |