HCID 18398261, compound → HCID 19600449, compound
Reaction equation
N[CH:2]1[CH2:7][CH2:6][CH:5]([C:8]2[CH:9]=[C:10]3[C:14](=[CH:15][CH:16]=2)[NH:13][CH:12]=[C:11]3[CH2:17][CH2:18][N:19]([CH3:21])[CH3:20])[CH2:4][CH2:3]1.NC1(C2C=C3C(=CC=2)NC=C3CCN(C)C)CCC=CC1>>[CH:5]1([C:8]2[CH:9]=[C:10]3[C:14](=[CH:15][CH:16]=2)[NH:13][CH:12]=[C:11]3[CH2:17][CH2:18][N:19]([CH3:20])[CH3:21])[CH2:4][CH2:3][CH2:2][CH2:7][CH2:6]1Participants
3
Procedure
5-(1-Aza-1-methylcyclohex-4-yl)-3-[2-(N,N-dimethylamino)ethyl]-1H-indole: (74%) from 5-(1-aza-1-methylcyclohex-3-en-yl)-3-[2-(N,N-dimethylamino)ethyl]-1H-indole (Example 16); HRMS-FAB+ for C18H28N3 : calculated MH+ :286.22833; found MH+ :286.22703.
Sources & evidence
- ORD record
- ord-d2fa5b3796bb49a7938e264780c7c639
- Source dataset
- uspto-grants-1999_12
- Patent number
- US05998438
Reaction notes
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