HRID610071

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID84347

Benzamide, 3-amino-N-phenyl-

C13H12N2O

结构：CCN1C(=O)C(C(=O)OC)c2cc(C3(CC)OCCO3)ccc21

HCID54561650

未命名化合物

PRODUCTS

生成物

结构：CCC(=O)c1ccc2c(c1)C(C(=O)Nc1cccc(C(=O)Nc3ccccc3)c1)C(=O)N2CC

HCID54503797

未命名化合物

PROCEDURE

实验过程

Prepared as in Example 1 from 1-ethyl-5-(2-ethyl-[1,3]dioxolan-2-yl)-2-oxo-2,3-dihydro-1H-indole-3-carboxylic acid methyl ester and 3-amino-N-phenyl-benzamide. Purified by flash-chromatography (chloroform/methanol, 20:1) followed by trituration in hexanes/ethyl acetate. mp 179-180° C.

WORKUP

后处理

customPurified by flash-chromatography (chloroform/methanol, 20:1)