Thiophenol → 4-Sulfanylbenzaldehyde

HRID 610100Notes

Reaction equation

[SH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[CH:9]([O:11]C)Cl>>[SH:1][C:2]1[CH:7]=[CH:6][C:5]([CH:9]=[O:11])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 7969Thiophenol

HCID 21004Methane, dichloromethoxy-

Product 1

HCID 109205784-Sulfanylbenzaldehyde

Procedure

The above reaction of Example 21A is repeated except that the starting materials are mercaptobenzene and dichloromethyl methylether. Using the same reaction conditions and techniques, there is obtained 4-mercaptobenzaldehyde.

Workup

customThe above reaction of Example 21A
customthe same reaction conditions and techniques

Sources & evidence

ORD record: ord-33138d93d39c43b998ae287067670ae3
Source dataset: uspto-grants-1999_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05998477

Reaction notes

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