HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride → HCID 67591911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride | HCID 23393 | — |
| Reactant | HCID 86745186 | HCID 86745186 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67591911 | HCID 67591911 | — |
Reaction Steps
By the method of Example 13, using flash chromatography with 40:9:1 CH2Cl2 :hexane:isopropanol as eluant and recrystallization from 1:1 toluene:hexane, the title product of Example 25 (0.37 g, 0.00128 mol) and 2-picolyl chloride were converted to present title product, 0.15 g (30%), m.p. 105-107° C. MS (m/e) calculated: 379.1424, found: 379.1394.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998451 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-e009e4204b654a58a460dff9d489f851 |
| Source note | uspto-grants-1999_12 |