HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 5-formyl-2-methoxybenzoate → 6-Benzyloxy-3-(4-methoxy-3-(methoxycarbonyl)benzylidene)-4-chromanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 5-formyl-2-methoxybenzoate | HCID 10856352 | — |
| Reactant | 6-(Benzyloxy)chroman-4-one | HCID 14422776 | — |
| Product | 6-Benzyloxy-3-(4-methoxy-3-(methoxycarbonyl)benzylidene)-4-chromanone | HCID 54022911 | — |
Reaction Steps
By the method of Example 44, 6-benzyloxy-4-chromanone (20.95 g) and 4-methoxy-3-methoxycarbonylbenzaldehyde were converted to present title product, 25.75 g (73%); tlc (19:1 CH2Cl2 :ether) Rf 0.70.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998451 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-c78a091d61f84eebbd0c32cf7da97415 |
| Source note | uspto-grants-1999_12 |