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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 610374Generated: October 30, 2026

Benzaldehyde → HCID 67592306, compound

https://huagongshe.com/reaction/610374

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantHCID 5146562HCID 5146562—
ProductHCID 67592306HCID 6759230663%

Reaction Steps

By the method of Example 146, 25.0 g (75.5 mmol) of 6-methoxy-1-(p-toluenesulfonyl)-2,3-dihydro-4(1H)-quinolinone (J. Am. Chem. Soc., Vol. 71, p. 1901, 1949) and 12.0 g (113 mmol) of benzaldehyde were converted to 20.0 g (63%) of present title product recrystallized from ether-hexane, m.p. 131-132° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05998451
Source datasetuspto-grants-1999_12
ORD IDord-d3bd3101562847bca86488f89485d4e6
Source noteuspto-grants-1999_12