HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-Hydroxybenzoate → HCID 19600740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-Hydroxybenzoate | HCID 88068 | — |
| Reactant | HCID 19600716 | HCID 19600716 | — |
| Product | HCID 19600740 | HCID 19600740 | — |
Reaction Steps
By the method of Example 72, 6-benzyloxy-3-bromo-4-chromanone (49.9 g, 0.15 mol) and methyl 3-hydroxy-benzoate (22.8 g, 0.15 mol) were converted to present title product purified by chromatography on silica gel using CH2Cl2 as eluant, 2.19 g; tlc Rf 0.22 (CH2Cl2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998451 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-bca3047905124167917fa003deb9a08c |
| Source note | uspto-grants-1999_12 |