HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → 6-Methoxy-3-(4-pyridyl)methylene-4-chromanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | 6-methoxy-3,4-dihydro-2H-1-benzopyran-4-one | HCID 4612168 | — |
| Product | 6-Methoxy-3-(4-pyridyl)methylene-4-chromanone | HCID 54062702 | — |
Reaction Steps
By the method of Example 1, 6-methoxy-4-chromanone (26.7 g, 0.15 mol) and pyridine-4-carbaldehyde were converted to present title product, 13.5 g; m.p. 170-171.5° C.; IR (KBr) 1675, 1616, 1598, 1552 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998451 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-2eb9c31c57e143eabed8d9137795ac13 |
| Source note | uspto-grants-1999_12 |