HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorothiophene-2-carbonyl Chloride → HCID 19601542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorothiophene-2-carbonyl Chloride | HCID 589223 | — |
| Reactant | 3-(1-Methyl-piperidin-4-yl)-1H-pyrrolo[3,2-b]pyridin-5-ylamine | HCID 10220230 | — |
| Product | HCID 19601542 | HCID 19601542 | 75% |
Reaction Steps
Beginning with 0.30 gm (1.3 mMol) 5-amino-3-(1-methylpiperidin-4-yl)pyrrolo[3,2-b]pyridine and 0.29 gm (1.56 mMol) 5-chloro-2-thiophenecarbonyl chloride, 0.36 gm (75%) of the title compound were prepared essentially by the procedure described in Example 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998622 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-f73ac0a07d1f4f0cad1305555ff8073c |
| Source note | uspto-grants-1999_12 |