HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → (E)-but-2-enedioic acid;copper
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Cupric acetate | HCID 8895 | — |
| Reactant | Fumaric Acid | HCID 444972 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (E)-but-2-enedioic acid;copper | HCID 90471545 | 33.4% |
Reaction Steps
0.58 g of fumaric acid was dissolved in a mixture solvent having 40 cm3 of methanol and 12 cm3 of formic acid. Then, under stirring at the normal temperature, into the above solution, a further solution in which 1.0 g of copper acetate was dissolved in 80 cm3 of methanol was dripped. After this solution was left still for a few days, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 0.3 g of fumaric acid copper was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998647 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-7bfb547bc0e74251bb8863eeadb38287 |
| Source note | uspto-grants-1999_12 |