HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → 2-Chloro-n-ethyl-6-(trimethylsilyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| Product | 2-Chloro-n-ethyl-6-(trimethylsilyl)benzamide | HCID 18630379 | — |
Reaction Steps
The compound of Example f (2.2 g, 0.012 mol) was reacted with TMSCl (3.91 g, 0.036 mol) using General Method A. The title compound was recrystallized from ether/hexanes as a solid. m.p. 105-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998466 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-3ccee119a5db4ef69be6f7bbf374dbbc |
| Source note | uspto-grants-1999_12 |