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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 611081Generated: November 1, 2026

Hydrochloric Acid → N,N-dimethyl-[5-(6-phenylhexyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine dihydrochloride

https://huagongshe.com/reaction/611081

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantN,N-Dimethyl-[5-(6-phenylhexyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl)amineHCID 19600160—
SolventMethanolHCID 887—
ProductN,N-dimethyl-[5-(6-phenylhexyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine dihydrochlorideHCID 19600159—

Reaction Steps

N,N-Dimethyl-[5-(6-phenylhexyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl)amine 0.199 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. After this mixture was concentrated, diethyl ether was added; the resulting solid was filtered and washed with diethyl ether to yield the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05998433
Source datasetuspto-grants-1999_12
ORD IDord-a4752d186eb04f1ca66c0b5ac188ad8e
Source noteuspto-grants-1999_12