HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19600120, compound → Methyl 4,5,6,7-tetrahydrofuro[2,3-c]pyridine-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19600120 | HCID 19600120 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 4,5,6,7-tetrahydrofuro[2,3-c]pyridine-2-carboxylate | HCID 19600098 | — |
Reaction Steps
A solution of 0.285 g (1.050 mmol) of methyl 6-benzyl-4,5,6,7-tetrahydrofuro[2,3-c]pyridine-2-carboxylate in 30 ml of methanol was hydrogenated at room temperature at atmospheric pressure over 0.2 g of 10% palladium-carbon (50% wet) overnight. After the catalyst was filtered off, the filtrate was evaporated under reduced pressure to yield the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05998433 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-bef794c704fe44a4bed37bbfb8a46dbd |
| Source note | uspto-grants-1999_12 |