HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 3-Benzyl-2-methyl-1,3-benzothiazol-3-ium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 2-Methylbenzothiazole | HCID 8446 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-Benzyl-2-methyl-1,3-benzothiazol-3-ium bromide | HCID 12792846 | — |
Reaction Steps
A solution of 2-methylbenzothiazole (5.0 g, 0.033 mol) and benzyl bromide (40 mL, 0.33 mol) in 250 mL of ethyl acetate was refluxed under nitrogen for 48 hours. Solid had formed. The mixture was filtered and washed with cold ethyl acetate to give 3-benzyl-2-methylbenzothiazol-3-ium bromide as a light yellow solid, mp 230-231° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001331 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-79ed2b70094d4f5d827b3e14d8a7c92e |
| Source note | uspto-grants-1999_12 |