Sodium;3-phenylprop-2-enoate → HCID 178525308, compound
Reaction equation
[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[Na+].[C:12]([O-:22])(=[O:21])[CH:13]=[CH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[Na+].[Cl-].[Zn+2:25].[Cl-]>>[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:12]([O-:22])(=[O:21])[CH:13]=[CH:14][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1.[Zn+2:25]Participants
4
Procedure
To the aqueous solution of sodium salicylate and the aqueous solution of sodium cinnamate was gradually added the aqueous solution of zinc chloride. The resulting mixture was stirred and the precipitate was filtered, washed with water, and dried to obtain a zinc cinnamate salicylate.
Workup
- filtrationthe precipitate was filtered
- washwashed with water
- customdried
Sources & evidence
- ORD record
- ord-528e5173f3d84e1b805af169d0aae51f
- Source dataset
- uspto-grants-1999_12
- Patent number
- US06001520
Reaction notes
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