HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-[(2-methoxy-2-oxoethyl)amino]benzoate → HCID 13693487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-[(2-methoxy-2-oxoethyl)amino]benzoate | HCID 5200104 | — |
| Reactant | Potassium cyanate | HCID 11378442 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13693487 | HCID 13693487 | — |
Reaction Steps
Monatsh. Chem. (1987) 118; pages 71-79 describes the reaction of methyl N-(methoxycarbonylmethyl)anthranilate with potassium cyanate in glacial acetic acid to give methyl 1,2,3,4-tetrahydro-2,4-dioxoquinazolin-1-ylacetate. Although 10 equivalents of potassium cyanate are employed, the yield is only 19%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001831 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-594da36ca34a4d7c84b8a810da038aca |
| Source note | uspto-grants-1999_12 |