HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide → HCID 178418303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide | HCID 53937500 | — |
| Reactant | Sodium hydrogen sulphide | HCID 86586439 | — |
| Product | HCID 178418303 | HCID 178418303 | 65.2% |
Reaction Steps
Using the procedure from Preparation 34, 5.8 g (17.9 mmol) of 4-chloro-2-phenyl-pyrimidine-5-carboxylic acid benzylamide was reacted with 5.1 g (72 mmol) of sodium hydrogen sulfide to give 3.75 g of the title compound, mp 189-193° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001863 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-a835807953bf4b7ea12570979ef5341d |
| Source note | uspto-grants-1999_12 |