HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 23287878, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | HCID 178418462 | HCID 178418462 | — |
| Product | HCID 23287878 | HCID 23287878 | 65.2% |
Reaction Steps
Using the procedure of Example 20, 33.0 g (96.2 mmol) of 4-mercapto-2-piperidin-1-yl-pyrimidine-5-carboxylic acid (2-pyridin-2-yl-ethyl)-amide were treated with 24.4 g (96.1 mmol) of iodine to give 21.4 g of the title compound after recrystallization from aqueous ethanol, mp 109-110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001863 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-48a2108743434d65aec088a4d8f03c64 |
| Source note | uspto-grants-1999_12 |