反应详情

This compound was synthesized from 7-(p-butylphenyl)-6-heptenoic acid (1.30 g, 5 mmol) by a hydrogenation reaction using Pd/C (130 mg). Crystallization (petroleum ether) afforded the product (1.19 g, 97%) as white crystals (mp 32-33° C.). IR: 3400-2500, 1718 cm-1 ; 1H-NMR:0.92 (t, 3 H), 1.35 (m, 6 H), 1.60 (m, 6 H), 2.32 (t, 2 H), 2.55 (m, 4 H), 7.02 (s, 4 H), 9.70 (bs, 1 H). Anal. Calcd. for C17H26O2 : C, 77.82, H, 9.99%; Found: C, 77.73, H, 10.01%.

1. customCrystallization (petroleum ether)