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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 611700Generated: October 30, 2026

HCID 15029695, compound → HCID 9807671, compound

https://huagongshe.com/reaction/611700

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15029695HCID 15029695—
SolventFormic AcidHCID 284—
ProductHCID 9807671HCID 980767162.9%

Reaction Steps

The butyl ester (70 mg; prepared in reference example 6) was dissolved in formic acid (5 ml). The solution was stirred for 5 hr. at room temperature. The reaction solution was evaporated to remove formic acid. The residue was purified by column chromatography on silica gel (ethyl acetate:methanol=10:1) to give the title compound (40 mg) of the present invention, having the following physical data.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06001877
Source datasetuspto-grants-1999_12
ORD IDord-2b91b96c95b14698b4f1a15b0d58d030
Source noteuspto-grants-1999_12