HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15029695, compound → HCID 9807671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15029695 | HCID 15029695 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 9807671 | HCID 9807671 | 62.9% |
Reaction Steps
The butyl ester (70 mg; prepared in reference example 6) was dissolved in formic acid (5 ml). The solution was stirred for 5 hr. at room temperature. The reaction solution was evaporated to remove formic acid. The residue was purified by column chromatography on silica gel (ethyl acetate:methanol=10:1) to give the title compound (40 mg) of the present invention, having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001877 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-2b91b96c95b14698b4f1a15b0d58d030 |
| Source note | uspto-grants-1999_12 |