HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Methoxy-6-methylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methoxy-6-methylbenzoic acid | HCID 273170 | — |
| Product | 2-Methoxy-6-methylbenzoyl chloride | HCID 12892675 | — |
Reaction Steps
A mixture of 1A (1.7 g, 10.2 mmol) and thionyl chloride (2 ml) is heated under reflux for 1 hour. The mixture is concentrated and the resulting benzoylchloride is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001883 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-450ca4c394d9487ebfe0cf542fbc9cb8 |
| Source note | uspto-grants-1999_12 |