HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 19598110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19598108 | HCID 19598108 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19598110 | HCID 19598110 | — |
Reaction Steps
A mixture of 4B (1.2 g, 4.6 mmol), dichloromethane (15 ml) and oxalyl chloride (1 ml) is stirred at room temperature for 2 hours. The mixture is concentrated and the resulting benzoylchloride is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001883 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-9bc39c3aa4e54477b2a4587843e940a9 |
| Source note | uspto-grants-1999_12 |