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HRID611721

反应详情

EQUATION

反应方程式

HRID 611721 的结构方程式

REACTANTS

反应物

3
结构：O=P12OP3(=O)OP(=O)(O1)OP(=O)(O2)O3
HCID14812

Phosphorus oxide (P4O10)

O10P4

结构：COc1cc(C)cc(OC)c1OC
HCID80922

3,4,5-Trimethoxytoluene

C10H14O3

结构：COc1cccc(C(F)(F)F)c1C(=O)O
HCID15017533

2-Methoxy-6-(trifluoromethyl)benzoic acid

C9H7F3O3

PRODUCTS

生成物

1
结构：COc1cc(C)c(C(=O)c2c(OC)cccc2C(F)(F)F)c(OC)c1OC
HCID17776999

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

65A (1.38 g, 0.00625 mol) is reacted with 3,4,5-trimethoxytoluene (1.14 g; 0.00625 mol) in the presence of P2O5 (5.0 g) and dichloromethane (100 ml) as described in Example 6 yielding white crystals, 1.68 g (69.8% ), mp 69-70° C.