HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxide (P4O10) → HCID 19598101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxide (P4O10) | HCID 14812 | — |
| Reactant | HCID 19598096 | HCID 19598096 | — |
| Reactant | 23550-92-7 | HCID 19598097 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19598101 | HCID 19598101 | — |
Reaction Steps
5-Chloro-2-methoxy-6-methylbenzoic acid (6.00 g, 0.03 mol) is reacted with 3,5-dimethoxy-4-propionyloxytoluene (6.73 g; 0.03 mol) in the presence of P2O5 (18.0 g) and dichloromethane (200 ml) as described in Example 6 yielding white crystals, 6.65 g (56.4% ), mp 150-151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001883 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-75cbc4866a1249a993f883c8910366c8 |
| Source note | uspto-grants-1999_12 |