HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Sulfate → HCID 22671389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Sulfate | HCID 6163 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19598113 | HCID 19598113 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22671389 | HCID 22671389 | — |
Reaction Steps
A mixture of 66B (1.15 g), potassium carbonate (1.0 g), diethylsulfate (0.54 g) and acetonitrile (20 ml) is heated to reflux for 3 hours. Upon cooling to room temperature water is added. The solid material is collected and the residue is re-crystallized from methanol yielding white crystals, 1.07 g (85.6% ), mp 131-132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06001883 |
| Source dataset | uspto-grants-1999_12 |
| ORD ID | ord-ed4e22848b82474b9f7f71baea625d75 |
| Source note | uspto-grants-1999_12 |